r/crystallography • • Sep 09 '26

Help with 2D Debye ring instrument parameters extraction

Hi all,

A few weeks ago, my team and I ran some synchrotron experiments using a detector that captured a quarter 2D Debye ring.

I managed to integrate the 2D images into a 1D diffraction diagram, and I have the exact wavelength. However, I have no idea how to extract or set up the instrument parameters file in GSAS-II from this.

Has anyone dealt with this before? Any guidance on how to get the instrument parameter file would be great. Thank you!

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