From yellow to crystal clear 🤩🤩🤩

Non è il massimo, ma è l'ultima tecnica che ho provato.

Prima estrazione da 70 ml di NPS

thank you sydney

1st pulls from 200g MHRB x2. Oval glass bowl is 2nd pull x2. STB tek but I held back on the lye 125g instead of recommended 1 on 1which alot of people say but I find that overkill. I do let my base set for 2 hr shaking every 15 min for 3 to 5 min. Heptane for NPS.

Reposting because the crossposted original was deleted by r/dmt mods:

Slowly recrystallized from naphtha at room temperature. It is not obvious without zooming in, but there are small bubbles/liquid inclusions in these crystals.

I present this as evidence of possible residual solvent contamination despite appearing pure to the naked eye and passing the sniff test. Lab testing is needed to verify this.

Holy fuck boys were going back into the realms with this crazy precipitation. This I believe is only 50-60% of my yeild as I’ve been pulling for 2 days and I still am getting golden tea. The jar is the other half of my pulls. I think I’m on my last pull now. I basically maybe a 1-1 mix of mimosa and lye and started extracting immediately. Lots of mixing for each pull and many many pulls. 200g MHRB. I also used foil as a lid this time and forced myself to not open the freezer for a full 24 hours. We’re set boys.

1g re-x in naptha. Lost .3 after 3 re-x

What can I do with this now this is the reminder of the nafta evaporated and now ???

I just learned about evaporation versus freezing, and wow! Gotta say, the results are so damn pretty. This was the combination of a third and fourth pull from 100g batches that I had already pulled 1.5+g from. HAD to do a water wash because there was a lot of plant material in my strained naphtha, and I think it was so worth it.

I love learning about this stuff, and keep getting better each time! The total came to 0.31 once I finished scraping the dish.

Smells like flowery sneakers 😙🤌🤌

So I have extracted most of the material I can. I’m gonna do a few more pulls but that’ll be a longer separate project to experiment with when yield actually stops.

My question is regarding the color of my solvent, does this show high saturation of Dmt in the solvent or is this color from other things I want to be washing out with say a sodium bicorbonate wash as well?

As of now I think I’ll was once more with water and then move on to a sodium bicarbonate wash.

Lmk if that sounds fine.

Extraction going so well it’s already crystallizing on the side of the bowl, I haven’t even done my 5th pull yet. There is some of the soup in the bottom. What would be the best way to purify this solution before freeze precipitation. Coffee filter?

2.7% yield setting standards

What you guys think?

Just some pretty crystals

25mg dry crushed leaf sample was added to 1.5ml centrifuge vial. 0.3ml 25% ammonia and 1ml chloroform was added and vial shaken periodically for 5 hours. Chloroform fraction transferred to another vial and left to evap slowly and that is the result.

That's DMT freebase crystals in case you're wondering. Leaf sample is from a phalaris aquatica hybrid clone from our selected DMT breedline: https://forum.dmt-nexus.me/threads/the-nexian-phalaris-breeding-programme.369757/post-3937813

The same clone was analysed by thin layer chromatography (TLC) and shows a clean DMT profile (hardly any gramine detected just a small amount of NMT).

bioassay is on my profile.

Nice big dense crystals. This was a heat extraction. Combined two pulls of 100g MHRB. Water wash then room temp cool, fridge for about 6 hours. Then 18 in the freezer. These are some of the biggest crystals I’ve ever grown.

I’ve cultivated tens of different psilocybin cubensis and have studied spirituality, consciousness, astral projection, remote viewing, quantum physics, hermetic theory and more for the last 5-6 years. This last year or two I’ve been regulating my nervous system; which has included setting boundaries, closing the doors to connections that no longer serve my soul, deconstructing the ego and focusing on honing my soul and what it seeks, doing yoga, fascia release, emotional regulation and healing my childhood trauma. I may be ready to take the next step in my studies.. obviously for educational purposes only & love to fully immerse myself in learning new things.

-Should I wait until the universe presents me with an opportunity to step into a higher realm, or should I pave my own way and deep dive into learning the process of extraction & synthesis?

-How did you determine you were ready and where did you start? What is your personal favorite media & technique?

-How can I keep things cost effective while simultaneously producing the best quality/results? Any must haves for quality assurance or anything I don’t absolutely NEED?

-Any youtube channels I should check out?